Crystallography Open Database





Information card for 7150580

7150579 << 7150580 >> 7150581

Preview

To alter the display settings, right click on the Jmol display.
Several types of unit cells can be loaded under the symmetry submenu.


Coordinates

7150580.cif

Structure parameters

Formula - C17 H24 Cl N -
Calculated formula - C17 H24 Cl N -
Title of publication Studies concerning the electrophilic amino-alkene cyclisation for the synthesis of bicyclic amines
Authors of publication Klein, Johannes E. M. N.; Müller-Bunz, Helge; Evans, Paul
Journal of publication Organic &amp; Biomolecular Chemistry
Year of publication 2009
Journal volume 7
Journal issue 5
Pages of publication 986 - 995
a 16.115 ± 0.002 Å
b 10.4898 ± 0.0013 Å
c 10.9685 ± 0.0014 Å
α 90°
β 121.095 ± 0.003°
γ 90°
Cell volume 1587.7 ± 0.3 Å3
Cell temperature 293 ± 2 K
Ambient diffraction temperature 293 ± 2 K
Number of distinct elements 4
Hermann-Mauguin symmetry space group C 1 2 1
Hall symmetry space group C 2y
Residual factor for all reflections 0.0517
Residual factor for observed reflections 0.0432
Weighted residual factors for the observed reflections 0.1006
Weighted residual factors for all reflections included in the refinement 0.1045
Goodness-of-fit parameter for observed reflections 1.063
Diffraction radiation wavelength 0.71073 Å
Diffraction radiation type MoKα
Has coordinates Yes
Has disorder No
Has Fobs No

Top of the page