Crystallography Open Database: Information card for 1501892

Structure parameters

Formula	C25 H36 N2 O3 S Si
Calculated formula	C25 H36 N2 O3 S Si
Title of publication	Total synthesis of (+)-condylocarpine, (+)-isocondylocarpine, and (+)-tubotaiwine.
Authors of publication	Martin, Connor L.; Nakamura, Seiichi; Otte, Ralf; Overman, Larry E.
Journal of publication	Organic letters
Year of publication	2011
Journal volume	13
Journal issue	1
Pages of publication	138 - 141
a	10.2168 ± 0.0005 Å
b	15.2722 ± 0.0007 Å
c	16.1196 ± 0.0007 Å
α	90°
β	100.054 ± 0.0006°
γ	90°
Cell volume	2476.6 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	6
Hermann-Mauguin symmetry space group	P 1 21/c 1
Hall symmetry space group	-P 2ybc
Residual factor for all reflections	0.0414
Residual factor for observed reflections	0.0349
Weighted residual factors for the observed reflections	0.0903
Weighted residual factors for all reflections included in the refinement	0.0951
Goodness-of-fit parameter for observed reflections	1.024
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Crystallography Open Database