Crystallography Open Database: Information card for 1501928

Structure parameters

Formula	C27 H22 O7
Calculated formula	C27 H22 O7
Title of publication	Rhodium-catalyzed tandem heterocyclization and carbonylative [(3+2)+1] cyclization of diyne-enones.
Authors of publication	Zhao, Wanxiang; Zhang, Junliang
Journal of publication	Organic letters
Year of publication	2011
Journal volume	13
Journal issue	4
Pages of publication	688 - 691
a	9.6288 ± 0.0004 Å
b	10.5846 ± 0.0004 Å
c	11.482 ± 0.0004 Å
α	75.515 ± 0.001°
β	80.586 ± 0.001°
γ	83.926 ± 0.001°
Cell volume	1115.17 ± 0.07 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	3
Hermann-Mauguin symmetry space group	P -1
Hall symmetry space group	-P 1
Residual factor for all reflections	0.0484
Residual factor for observed reflections	0.0401
Weighted residual factors for the observed reflections	0.1053
Weighted residual factors for all reflections included in the refinement	0.1146
Goodness-of-fit parameter for observed reflections	1.052
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Crystallography Open Database