Crystallography Open Database: Information card for 7000201

Structure parameters

Formula	C48 H35 N3 Os P2
Calculated formula	C48 H35 N3 Os P2
Title of publication	Tricyanovinylalkynyl‒metal complexes: synthesis and some reactions
Authors of publication	Bruce, Michael I.; Burgun, Aléxandre; Kramarczuk, Kathy A.; Nicholson, Brian K.; Parker, Christian R.; Skelton, Brian W.; White, Allan H.; Zaitseva, Natasha N.
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	1
Pages of publication	33 - 36
a	11.4883 ± 0.0009 Å
b	17.556 ± 0.002 Å
c	19.604 ± 0.002 Å
α	90°
β	100.126 ± 0.002°
γ	90°
Cell volume	3892.3 ± 0.7 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Hermann-Mauguin symmetry space group	P 1 21/n 1
Hall symmetry space group	-P 2yn
Residual factor for all reflections	0.0626
Residual factor for observed reflections	0.0299
Weighted residual factors for the observed reflections	0.0535
Weighted residual factors for all reflections included in the refinement	0.0585
Goodness-of-fit parameter for observed reflections	0.884
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Crystallography Open Database