Crystallography Open Database: Information card for 7000406

Structure parameters

Formula	C23 H16 Br2 N4
Calculated formula	C23 H16 Br2 N4
Title of publication	Direct synthesis of a new class of N,N,N ligands based on 1,2-dihydro-1,10-phenanthroline backbone and their coordination to Pd complexes
Authors of publication	Rangheard, Claudine; Proriol, David; Olivier-Bourbigou, Hélène; Braunstein, Pierre
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	5
Pages of publication	770 - 772
a	10.5388 ± 0.0007 Å
b	19.5573 ± 0.0008 Å
c	10.6246 ± 0.0007 Å
α	90°
β	112.491 ± 0.002°
γ	90°
Cell volume	2023.3 ± 0.2 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Hermann-Mauguin symmetry space group	P 1 21/c 1
Hall symmetry space group	-P 2ybc
Residual factor for all reflections	0.0822
Residual factor for observed reflections	0.0444
Weighted residual factors for the observed reflections	0.0892
Weighted residual factors for all reflections included in the refinement	0.0973
Goodness-of-fit parameter for observed reflections	0.979
Diffraction radiation probe	x-ray
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Crystallography Open Database