Crystallography Open Database: Information card for 7000417

Structure parameters

Formula	C21 H25 Al Li N3 O
Calculated formula	C21 H25 Al Li N3 O
Title of publication	Metal and ligand substitution of the aluminium tris-pyridyl ligands [RAl(2-py′)3]− (R = Et, nBu, sBu, tBu; 2-py′ = 2-pyridyl, 3-methyl-2-pyridyl, 5-methyl-2-pyridyl, 6-methyl-2-pyridyl)
Authors of publication	Bullock, Thomas H.; Chan, Wesley T. K.; Eisler, Dana J.; Streib, Manuel; Wright, Dominic S.
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	6
Pages of publication	1046 - 1054
a	8.8009 ± 0.0018 Å
b	9.8739 ± 0.0002 Å
c	12.8545 ± 0.0003 Å
α	78.9146 ± 0.0009°
β	71.2169 ± 0.0009°
γ	76.9896 ± 0.001°
Cell volume	1021.7 ± 0.2 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	6
Hermann-Mauguin symmetry space group	P -1
Hall symmetry space group	-P 1
Residual factor for all reflections	0.0588
Residual factor for observed reflections	0.0416
Weighted residual factors for the observed reflections	0.0969
Weighted residual factors for all reflections included in the refinement	0.107
Goodness-of-fit parameter for observed reflections	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Crystallography Open Database